Controlled batch distillation in a vacuum and at atmospheric pressure

Apply a single-fluid industrial heating process


GENERAL SPECIFICATIONS


  • 10 L storage tank.
  • DN 200, 6 L, boiler. SS resistance.
  • DN 50 glass column, packing,3 SS trays, removable insulation.
  • Glass reflux head.
  • SS coil, glass condenser.
  • 2 glass vessel , 1 L.
  • Cooling water circuit

Instrumentation

  • 5 temperature probe.
  • Flowmeter with safety.
  • Level detector.

Hydrodynamic study of the column

Determine overflooding conditions

Determine packing factor

 

Influence of operating parameters

Reflux ratio, differential pressure of column

Control of head temperature

 

Operate a batch process

Materials balances

Thermal balance

Yield, productivity