Synthesis, dissolution, crystallization with concentration by evaporation

 


GENERAL SPECIFICATIONS


Evaporation concentration 

  • 20 L polyethylene tank.
  • Dosing pump.
  • ND 200 glass reactor, 10 L, glass double jacket, 0,1m2 stainless steel coil.
  • Cover, ND200.
  • Stirring.
  • Reflux ratio head with manual setting.
  • ND 50 glass condenser, SS coil.
  • SS condensate coolant.
  • Graduated glass receiver, 5 L.
  • 1 L funnel, glass, graduated.

Cristallization 

  • ND 150 glass crystallizer, 5 L capacity.
  • Cover with loading hatch for feeding.
  • SS coil with setting valve.
  • Stirring.
  • Cold water circuitry
  • Control vacuum circuitry

 

Dim : 220 x 100 x 230 cm – 200 kg
SS tubular framework 40 x 40mm

 

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Study the evaporation process

Mass balance on the evaporator

Thermal balance on condenser

 

Study of crystallisation by cooling process

Seeding of supersaturated solution.

Monitoring of cooling rate by thermal balance

Mass balance on crystal production

 

Implement a batch process and a continuous process