Synthesis, dissolution, crystallization with concentration by evaporation
- 20 L polyethylene tank.
- Dosing pump.
- ND 200 glass reactor, 10 L, glass double jacket, 0,1m2 stainless steel coil.
- Cover, ND200.
- Reflux ratio head with manual setting.
- ND 50 glass condenser, SS coil.
- SS condensate coolant.
- Graduated glass receiver, 5 L.
- 1 L funnel, glass, graduated.
- ND 150 glass crystallizer, 5 L capacity.
- Cover with loading hatch for feeding.
- SS coil with setting valve.
- Cold water circuitry
- Control vacuum circuitry
Study the evaporation process
Mass balance on the evaporator
Thermal balance on condenser
Study of crystallisation by cooling process
Seeding of supersaturated solution.
Monitoring of cooling rate by thermal balance
Mass balance on crystal production