Study of 2 different distillations

Study of the coupling of the 2 columns


GENERAL SPECIFICATIONS


  • Metering pump.
  • Electric pre-heater.
  • Feeding manifold.
  • Jacketed azeotropic settler.
  • Multiknit column.
  • Bubble caps column.

Each column is equipped with

  • Glass heater, 6 L.
  • Electromagnetic reflux divider.
  • Glass condenser, SS coil.
  • Glass receiver, graduated, 1 L.
  • Removable insulation and three SS sampling plates.

Instrumentation

  • Temperature probes Pt100Ω.
  • 2 differential pressure transmitter.
  • 2 flowmeters.
  • 3 level sensors
  • 1 pressure relief valve.
  • 2 thermostats.

 

Dim : 262 x 70 x 300 cm – 370 kg
SS tubular framework 40 x 40mm

 

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Distillation or rectification

The distillation process separates several volatile liquids, simple or complex mixtures,

by a series of vaporisation and condensation steps.

A number of liquids may be separated in this way if their boiling points are sufficiently different.

Continuous distillation separates a mixture into fractions: a volatile fraction, the distillate extracted

at the column head and a heavy fraction, the residue extracted at the bottom of the column.

 

Study of 2 different distillations

Batch distillation with bubble cap column

Continuous distillation with packed column

 

Study of the coupling of the 2 columns

Ternary Distillation

Hetero-azeotropic distillation