Operate a continuous distillation process
Operate a batch distillation process
GENERAL SPECIFICATIONS
- Metering pump.
- Electrical pre-heater.
- 3 feeding level on the column.
- Glass shell heater equipped with a resistance overflow tube.
- Glass Column with Multiknit packing and SS Sampling flange.
- Glass reflux head, with reflux dividing solenoid valve.
- SS & glass coil condenser.
- 2 graduated glass receivers.
Safety
– Venting thermostate.
– Pressure relief on the preheater.
Instrumentation
- Temperature probes Pt100Ω.
- Differential pressure transmitter.
- Flowmeter.
- Level sensor.
- Touch screen with data acquisition.
Dim : 150 x 70 x 240 cm – 150 kg
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Distillation or rectification:
The distillation process separates several volatile liquids, simple or complex mixtures,
by a series of vaporisation and condensation steps.
A number of liquids may be separated in this way if their boiling points are sufficiently different.
Continuous distillation separates a mixture into fractions: a volatile fraction, the distillate
extracted at the column head and a heavy fraction, the residue extracted at the bottom of the column.
Characterization of a distillation efficiency
Determination of the theoretical
Number of plates
Influence of the operating parameters
Preheating temperature
Feed rate
Reflux ratio
Column pressure drop
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