Cooling by water circulation inside the double jacket

Multipurpose unit for :

Liquid-liquid mixture

Solid-Liquid dissolution

Evaporation, concentration

Reaction, synthesis

Distillation

Decantation, crystallization

 

Heating by steam generator


GENERAL SPECIFICATIONS


  • Jacketed SS vessel, and SS flat cover.
  • Variable speed stirrer.
  • Glass feeding vessel.
  • Glass distillation column, SS Multiknit packing.
  • Reflux divider with PTFE pneumatic valve.
  • Glass calendar condenser and SS coil.
  • Glass azeotropic decanter , glass double jacket.
  • SS distillate cooler.
  • Two graduated glass receivers, 2L, three ways selecting valve, setting, vent and draining valves.
  • Vacuum circuit with vacuum trap.
  • Vacuum pump.
  • Cold water circuit.
  • Steam circuit : with solenoid valve, insulated pipes.
  • Steam generator.

Instrumentation

  • 5 temperature probes Pt100Ω.
  • 3 flowmeters:.
  • Vacuum manometer.
  • Solenoid valve on steam circuit.

Safety

  • Discharge check valve.
  • Motor coupling and reactor protection.
  • Steam cut off in case of emergency.
Categories: Reference:

Operator training to monitor the process

Unit placed under vacuum

Compliance with procedures

Loading through the dropping funnel

Receivers draining under vacuum

Phenomena viewing

Synoptic follow

Curves using

Unit cleaning

Handling report

 

Follow – up of reaction kinetics

Kinetic, material balance, reaction yield

 

Separation of the products

By distillation, decantation or crystallization