Cooling by water circulation inside the double jacket
Multipurpose unit for :
Heating by steam generator
- Jacketed SS vessel, and SS flat cover.
- Variable speed stirrer.
- Glass feeding vessel.
- Glass distillation column, SS Multiknit packing.
- Reflux divider with PTFE pneumatic valve.
- Glass calendar condenser and SS coil.
- Glass azeotropic decanter , glass double jacket.
- SS distillate cooler.
- Two graduated glass receivers, 2L, three ways selecting valve, setting, vent and draining valves.
- Vacuum circuit with vacuum trap.
- Vacuum pump.
- Cold water circuit.
- Steam circuit : with solenoid valve, insulated pipes.
- Steam generator.
- 5 temperature probes Pt100Ω.
- 3 flowmeters:.
- Vacuum manometer.
- Solenoid valve on steam circuit.
- Discharge check valve.
- Motor coupling and reactor protection.
- Steam cut off in case of emergency.
Operator training to monitor the process
Unit placed under vacuum
Compliance with procedures
Loading through the dropping funnel
Receivers draining under vacuum
Follow – up of reaction kinetics
Kinetic, material balance, reaction yield
Separation of the products
By distillation, decantation or crystallization