Study of the batch distillation
Glass spherical boiler
Perforate plates column
Internal reflux
GENERAL SPECIFICATIONS
- Glass boiler vessel, with draining valve.
- Heating mantle, protection by insulation and SS sheet.
- Distillation column with perforated plates, sampling valve.
- Glass reflux divider, glass distillate draining out by a solenoid acting a magnetic valve.
- Glass condenser, glass coil.
- SS cooler.
- Glass distillate receiver.
- Cool water circuit.
Instrumentation
- Temperature probes Pt100Ω.
- Flowmeter.
Dim : 135 x 60 x 145 cm – 60 kg
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Influence of operating parameters
Reflux ratio, boiler heating capacity, quality of mixture to be distilled
Batch distillation
Materials balance
Monitoring of liquid-vapor equilibrium and temperatures
Yield, productivity