Organic and inorganic synthesis in a corrosive solutions
- Spherical glass flask, 10 L, heating mantel 2 kW.
- Silicone mantle for top protection.
- Lifting table.
- Glass lid with connections for temperature probe, feeding orifice, stirring bearing box, condenser inlet, reactive flow.
- Stirrer, variable speed, PTFE coated SS shaft, mobile PTFE three-paddle helix.
- Glass condenser.
- Glass graduated receiver, capacity 1 L with PTFE draining valve, and connection to vacuum circuit by PTFE flexible.
- Graduated glass feeding funnel, capacity 1 L.
- Temperature probe Pt100Ω.
- Digital thermometer.
Reactions under reflux
Concentration under reduced pressure and atmospheric pressure