Reactional calorimetry study

Continuous process


GENERAL SPECIFICATIONS


  • Double jacketed glass reactor, 1 L,
  • Double jacketed lid.
  • Variable rate stirrer.
  • Feeding funnel in glass.
  • High flow rate cooling group.
  • Calorimetric data calculation software.

Instrumentation

  • Pressure transmitter.
  • Flow rate transmitter.
  • Temperature probes Pt100Ω.

 

Dim : 130 x 75 x 200 cm – 100 kg
Aluminum profile framework

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Determination of massic heats and reaction enthalpy

Calculation from calorimetry software results

Calibration

 

Experiments with acetic anhydride

 

Influence of reaction parameters